{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

Base Information

Chemical Name:{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride
CAS No.:923975-92-2
Molecular Formula:C₁₇H₁₉ClN₂O₃
Molecular Weight:334.802
Hs Code.:

Synonyms:{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

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Chemical Property of {3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

Chemical Property:

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Technology Process of {3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

There total 3 articles about {3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 923975-91-1
{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetic acid

: 923975-92-2
{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 923975-89-7
3-[4-(methyloxy)phenyl]-1,4-diazaspiro[4.5]dec-3-en-2-one

: 923975-92-2
{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 160 h / Heating / reflux

2.1: sodium hydroxide / ethanol; water / 16 h / Heating / reflux

2.2: pH < 7

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

With sodium hydroxide; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In ethanol; dichloromethane; water; acetone;

Reference yield:

: 923975-90-0
ethyl {3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetate

: 923975-92-2
{3-[4-(methyloxy)phenyl]-2-oxo-1,4-diazaspiro[4.5]dec-3-en-1-yl}acetyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol; water / 16 h / Heating / reflux

1.2: pH < 7

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

With sodium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In ethanol; dichloromethane; water;