C₁₃H₁₉F₂NOSi

Base Information

• Chemical Name: C₁₃H₁₉F₂NOSi
• CAS No.: 1252030-16-2
• Molecular Formula: C₁₃H₁₉F₂NOSi
• Molecular Weight: 271.382
• Mol file: 1252030-16-2.mol

Synonyms:C₁₃H₁₉F₂NOSi

Chemical Property of C₁₃H₁₉F₂NOSi

Chemical Property:

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Technology Process of C₁₃H₁₉F₂NOSi

There total 1 articles about C₁₃H₁₉F₂NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2,2-difluoro-4-iodo-4-(trimethylsilyl)butanal (1252030-07-1) + aniline (62-53-3) → C13H19F2NOSi (1252030-16-2)

Guidance literature:

In acetonitrile; at 20 ℃; for 8h;

DOI:10.5012/bkcs.2010.31.01.031

Reference yield: 78.0%

C13H19F2NOSi (1252030-16-2) → 1-phenyl-3-fluoropyrrole (148541-80-4)

Guidance literature:

With potassium fluoride; In dimethyl sulfoxide; at 100 ℃; for 15h;

DOI:10.5012/bkcs.2010.31.01.031

upstream raw materials:

2,2-difluoro-4-iodo-4-(trimethylsilyl)butanal

aniline

Downstream raw materials:

1-phenyl-3-fluoropyrrole

Refernces