Technology Process of C22H22O5
There total 9 articles about C22H22O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
ethyl acetate;
at 80 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/ja203642n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere
2: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere
With
chloro-trimethyl-silane; sodium cyanoborohydride; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; ethyl acetate; acetonitrile;
DOI:10.1021/ja203642n
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium chlorite; sodium phosphate monobasic monohydrate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 °C
2: sulfuric acid / 0 - 20 °C / Inert atmosphere
3: toluene-4-sulfonic acid / tetrahydrofuran / 80 °C / Inert atmosphere
4: chloro-trimethyl-silane; sodium cyanoborohydride / acetonitrile / 0 °C / Inert atmosphere; Heating
5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere
With
sodium chlorite; chloro-trimethyl-silane; sodium phosphate monobasic monohydrate; sulfuric acid; sodium cyanoborohydride; toluene-4-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; 2-methyl-but-2-ene; water; ethyl acetate; acetonitrile; tert-butyl alcohol;
1: Pinnick oxidation;
DOI:10.1021/ja203642n
