C₂₃H₂₉NSi

Base Information

• Chemical Name: C₂₃H₂₉NSi
• CAS No.: 1016970-56-1
• Molecular Formula: C₂₃H₂₉NSi
• Molecular Weight: 347.575
• Mol file: 1016970-56-1.mol

Synonyms:C₂₃H₂₉NSi

Chemical Property of C₂₃H₂₉NSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₂₉NSi

There total 2 articles about C₂₃H₂₉NSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-N-benzyl-2-methylprop-2-en-1-imine + 1-(trimethylsilyl)-3-phenylprop-1-yne (31683-47-3) → C23H29NSi (1016970-56-1)

Guidance literature:

[RhCl(coe)2]2; In toluene; at 100 ℃; for 4h;

DOI:10.1021/ja7104784

Reference yield:

CH2C(CH3)CHNBn (27760-62-9) + 1-(trimethylsilyl)-3-phenylprop-1-yne (31683-47-3) → C23H29NSi (1016970-56-1)

Guidance literature:

With chlorobis(cyclooctene)rhodium(I) dimer; diethyl-{4-dimethylamino-phenyl}-phosphine; In toluene; at 100 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja312311k

Reference yield:

C23H29NSi (1016970-56-1) → 3-benzyl-5-methylpyridine

Guidance literature:

C₂₃H₂₉NSi; With air; palladium on activated charcoal; In 2,2,2-trifluoroethanol; toluene; at 23 ℃; for 16h;

With hydrogen; palladium on activated charcoal; In 2,2,2-trifluoroethanol; toluene; at 20 ℃; for 12h; Further stages.;

DOI:10.1021/ja7104784

upstream raw materials:

1-(trimethylsilyl)-3-phenylprop-1-yne

CH₂C(CH₃)CHNBn

Downstream raw materials:

C₂₀H₂₃N