5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

Base Information

Chemical Name:5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline
CAS No.:127999-82-0
Molecular Formula:C₂₀H₁₈N₂O₂
Molecular Weight:318.375
Hs Code.:

5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopent<c>isoquinoline

Synonyms:5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

Chemical Property:

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Technology Process of 5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

There total 4 articles about 5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 127999-70-6
methyl 5-cyano-5-(2-cyanophenyl)-5-phenylpentanoate

: 127999-82-0
5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

Guidance literature:: With potassium tert-butylate; In chlorobenzene;
DOI:10.1021/jo00303a012

Reference yield:

: 873-32-5
2-Chlorobenzonitrile

: 127999-82-0
5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.) DMF, 1 h, 2.) 30 deg C

2: 81 percent / potassium tert-butoxide / chlorobenzene

With potassium tert-butylate; In chlorobenzene;
DOI:10.1021/jo00303a012

Reference yield:

: 4897-84-1
Methyl 4-bromobutyrate

: 127999-82-0
5-amino-3-(methoxycarbonyl)-9b-phenyl-2,9b-dihydro-1H-cyclopentisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.) DMF, 1 h, 2.) 30 deg C

2: 81 percent / potassium tert-butoxide / chlorobenzene

With potassium tert-butylate; In chlorobenzene;
DOI:10.1021/jo00303a012