2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

Base Information

Chemical Name:2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro
CAS No.:127257-39-0
Molecular Formula:C₂₂H₂₆O₂S₂
Molecular Weight:386.579
Hs Code.:

2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro<cyclohexane-1,1'-oxirane>

Synonyms:2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

Chemical Property:

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Technology Process of 2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

There total 3 articles about 2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(1-Benzenesulfinyl-4-phenylsulfanyl-butyl)-cyclohexanol

: 127257-39-0
2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; tert-butyl alcohol; for 0.166667h; Yield given; Ambient temperature;
DOI:10.1021/jo00299a052

Reference yield:

: 127279-34-9
1-chloro-4-(phenylthio)butyl phenyl sulfoxide

: 127257-39-0
2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / THF, - 60 deg C, 1) 15 min, 2) 5 min

2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / 0.17 h / Ambient temperature

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1021/jo00299a052

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 127257-39-0
2'-(phenylsulfinyl)-2'-(3-(phenylthio)propyl)spiro

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / THF, - 60 deg C, 1) 15 min, 2) 5 min

2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / 0.17 h / Ambient temperature

With potassium tert-butylate; lithium diisopropyl amide; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1021/jo00299a052