hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

Base Information

Chemical Name:hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate
CAS No.:152809-61-5
Molecular Formula:C₁₉H₂₁N₃O₉
Molecular Weight:435.39
Hs Code.:

Synonyms:hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

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Chemical Property of hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

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Technology Process of hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

There total 3 articles about hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.5%

: 152809-60-4
4-nitrooxybutyl 2-cyanoethyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

: 152809-61-5
hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

Guidance literature:: With sodium hydroxide; In acetone; for 2h; Ambient temperature;
DOI:10.1248/cpb.41.1049

Reference yield:

: 152809-59-1
4-bromobutyl acetoacetate

: 152809-61-5
hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 79.4 percent / silver nitrate / acetonitrile / 10 h / Ambient temperature

2: 54.3 percent / propan-2-ol / 3 h / Heating

3: 83.5 percent / 5 N NaOH / acetone / 2 h / Ambient temperature

With sodium hydroxide; silver nitrate; In isopropyl alcohol; acetone; acetonitrile;
DOI:10.1248/cpb.41.1049

Reference yield:

: 152809-62-6
4-nitrooxybutyl acetoacetate

: 152809-61-5
hydrogen 4-nitrooxybutyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydro-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 54.3 percent / propan-2-ol / 3 h / Heating

2: 83.5 percent / 5 N NaOH / acetone / 2 h / Ambient temperature

With sodium hydroxide; In isopropyl alcohol; acetone;
DOI:10.1248/cpb.41.1049