dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Base Information

Chemical Name:dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate
CAS No.:1310049-18-3
Molecular Formula:C₁₉H₂₁N₂O₄P
Molecular Weight:372.361
Hs Code.:

Synonyms:dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Suppliers and Price of dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

There total 6 articles about dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1310049-15-0
methyl (E)-2-((indolin-1-ylimino)methyl)benzoate

: 756-79-6
dimethyl methane phosphonate

: 1310049-18-3
dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

methyl (E)-2-((indolin-1-ylimino)methyl)benzoate; In tetrahydrofuran; hexane; at -78 ℃; for 4h;
DOI:10.1021/jo200896y

Reference yield:

: 496-15-1
1-indoline

: 1310049-18-3
dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; sodium nitrite / water

2.1: lithium aluminium tetrahydride / tetrahydrofuran

3.1: methanol; ethanol / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

4.2: 4 h / -78 °C

With lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; sodium nitrite; In tetrahydrofuran; methanol; ethanol; hexane; water;
DOI:10.1021/jo200896y

Reference yield:

: 7633-56-9
N-aminoindoline

: 1310049-18-3
dimethyl (E)-2-(2-((indolin-1-ylimino)methyl)phenyl)-2-oxoethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; ethanol / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 4 h / -78 °C

With n-butyllithium; In tetrahydrofuran; methanol; ethanol; hexane;
DOI:10.1021/jo200896y