(+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone

Base Information

• Chemical Name: (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone
• CAS No.: 860606-17-3
• Molecular Formula: C₁₅H₁₃F₃N₂O₂
• Molecular Weight: 310.276

Synonyms:(+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone

Chemical Property of (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone

Chemical Property:

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Technology Process of (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone

There total 7 articles about (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-Phenyl-(2,2,2-trifluoro-acetylamino)-acetyl chloride + N-Methylpyrrole (96-54-8) → (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone (860606-17-3)

Guidance literature:

With aluminium trichloride; In dichloromethane; at -5 ℃; for 2h;

DOI:10.1021/jm701378e

Reference yield:

(S)-Phenyl-(2,2,2-trifluoro-acetylamino)-acetyl chloride + N-Methylpyrrole (96-54-8) → (-)-(R)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone (860606-19-5) + (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone (860606-17-3)

Guidance literature:

With aluminium trichloride; In dichloromethane; at -5 ℃; for 2h;

DOI:10.1021/jm050172c

Reference yield:

(R)-Phenyl-(2,2,2-trifluoro-acetylamino)-acetyl chloride + N-Methylpyrrole (96-54-8) → (-)-(R)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone (860606-19-5) + (+)-(S)-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-2-[N-(trifluoroacetyl)amino]ethanone (860606-17-3)

Guidance literature:

With aluminium trichloride; In dichloromethane; at -5 ℃; for 2h;

DOI:10.1021/jm050172c

upstream raw materials:

N-Methylpyrrole

(+)-(S)-N-trifluoroacetylphenylglycine

(S)-2-phenylglycine

(R)-phenylglycine

Downstream raw materials:

2-amino-1-(1-methyl-1H-pyrrol-2-yl)-2-phenyl-ethanone

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