[5-(((CH₃)3CCH₂CONHC₅H₃NNHCO)2C₆H₃NHCOCH₂OC₆H₄)-10,15,20-(p-tert-butylphenyl)3C₂₀H₈N₄]SnCl₂

Base Information

• Chemical Name: [5-(((CH₃)3CCH₂CONHC₅H₃NNHCO)2C₆H₃NHCOCH₂OC₆H₄)-10,15,20-(p-tert-butylphenyl)3C₂₀H₈N₄]SnCl₂
• CAS No.: 1004995-29-2
• Molecular Formula: C₈₈H₈₉Cl₂N₁₁O₆Sn
• Molecular Weight: 1586.36

Synonyms:[5-(((CH₃)3CCH₂CONHC₅H₃NNHCO)2C₆H₃NHCOCH₂OC₆H₄)-10,15,20-(p-tert-butylphenyl)3C₂₀H₈N₄]SnCl₂

Chemical Property of [5-(((CH₃)3CCH₂CONHC₅H₃NNHCO)2C₆H₃NHCOCH₂OC₆H₄)-10,15,20-(p-tert-butylphenyl)3C₂₀H₈N₄]SnCl₂

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Technology Process of [5-(((CH₃)3CCH₂CONHC₅H₃NNHCO)2C₆H₃NHCOCH₂OC₆H₄)-10,15,20-(p-tert-butylphenyl)3C₂₀H₈N₄]SnCl₂

There total 1 articles about [5-(((CH₃)3CCH₂CONHC₅H₃NNHCO)2C₆H₃NHCOCH₂OC₆H₄)-10,15,20-(p-tert-butylphenyl)3C₂₀H₈N₄]SnCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

5-(p-carboxymethylphenyl)-10,15,20-tris(p-tert-butylphenyl)porphyrin + tin(ll) chloride → [5-(((CH3)3CCH2CONHC5H3NNHCO)2C6H3NHCOCH2OC6H4)-10,15,20-(p-tert-butylphenyl)3C20H8N4]SnCl2 (1004995-29-2)

Guidance literature:

In acetic acid; addn. of tin compd. to soln. of porphyrin deriv. in acetic acid, heatingat reflux for 15 h; evapn., chromy. (CH2Cl2/methanol (9:1)), concn., recrystn. (pentane), NMR;

DOI:10.1021/ja075751g

Reference yield:

((CH3)3COCOCH2CH2)3CNHCOCH2CH2CH2OCOC(C60)COO(CH2)3C3H2N3O3 (943297-73-2) + [5-(((CH3)3CCH2CONHC5H3NNHCO)2C6H3NHCOCH2OC6H4)-10,15,20-(p-tert-butylphenyl)3C20H8N4]SnCl2 (1004995-29-2) → [5-(((CH3)3CCH2CONHC5H3NNHCO)2C6H3NHCOCH2OC6H4)-10,15,20-(p-tert-butylphenyl)3C20H8N4]SnCl2*C95H54N4O14

Guidance literature:

In dichloromethane; addn. of fullerene deriv. to CH2Cl2 soln. of tin porphyrin deriv.; not isolated, fluorescence spectroscopy;

DOI:10.1021/ja075751g

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