3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol

Base Information

• Chemical Name: 3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol
• CAS No.: 135303-94-5
• Molecular Formula: C₃₁H₃₂O₇
• Molecular Weight: 516.591
• Mol file: 135303-94-5.mol

Synonyms:3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol

Chemical Property of 3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol

There total 2 articles about 3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 3-<4-<2-<3,4-dimethoxy-2-(3-methoxycarbonylphenoxy)phenyl>ethyl>phenoxy>-4-methoxybenzoate (135303-93-4) → 3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol (135303-94-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

methyl 3-<4-<2-<3,4-dimethoxy-2-(3-methoxycarbonylphenoxy)phenyl>vinyl>phenoxy>-4-methoxybenzoate (135303-92-3,135303-99-0) → 3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol (135303-94-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / H₂ / Pd/C / ethyl acetate; ethanol

2: 95 percent / LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;

Reference yield: 74.0%

3-<4-<2-<(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzylalcohol (135303-94-5) → 3-<4-<2-<(3-bromomethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzyl bromide (135327-84-3)

Guidance literature:

With phosphorus tribromide; In benzene;

upstream raw materials:

methyl 3-<4-<2-<3,4-dimethoxy-2-(3-methoxycarbonylphenoxy)phenyl>ethyl>phenoxy>-4-methoxybenzoate

methyl 3-<4-<2-<3,4-dimethoxy-2-(3-methoxycarbonylphenoxy)phenyl>vinyl>phenoxy>-4-methoxybenzoate

Downstream raw materials:

3-<4-<2-<(3-bromomethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4-methoxybenzyl bromide