tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate

Base Information

Chemical Name:tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate
CAS No.:891269-71-9
Molecular Formula:C₂₈H₃₅N₃O₃
Molecular Weight:461.604
Hs Code.:

Synonyms:tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate

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Chemical Property of tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate

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Technology Process of tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate

There total 1 articles about tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 891269-62-8
(2S)-2-{[(tert-butoxy)carbonyl]amino}-8-oxononanoic acid

: 1484-50-0
desyl bromide

: 891269-70-8
tert-Butyl [(1S)-1-(4,5-diphenyl-1,3-oxazol-2-yl)-7-oxooctyl]carbamate

: 891269-71-9
tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate

Guidance literature:: (2S)-2-{[(tert-butoxy)carbonyl]amino}-8-oxononanoic acid; With caesium carbonate; In ethanol; at 20 ℃; for 0.5h;

desyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

With ammonium acetate; In xylene; at 150 ℃; for 1.5h; Heating / reflux;

Reference yield:

: 891269-70-8
tert-Butyl [(1S)-1-(4,5-diphenyl-1,3-oxazol-2-yl)-7-oxooctyl]carbamate

: 891269-71-9
tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate

: 71985-80-3,71235-92-2
1-methylpiperidine-4-carboxylic acid hydrochloride

: 76-05-1
trifluoroacetic acid

: 891269-67-3
4-({[(1S)-1-(4,5-diphenyl-1,3-oxazol-2-yl)-7-oxooctyl]amino}-carbonyl)-1-methylpiperidinium trifluoroacetate

: (4-{[(1S)-1-(4,5-diphenyl-1H-imidazol-1-ium-2-yl)-7-oxooctyl]amino}carbonyl)-1-methyl piperidinium bis(trifluoroacetate)

Guidance literature:: tert-Butyl [(1S)-1-(4,5-diphenyl-1,3-oxazol-2-yl)-7-oxooctyl]carbamate; tert-butyl [(1S)-1-(4,5-diphenyl-1,3-imidazol-2-yl)-7-oxooctyl]carbamate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

1-methylpiperidine-4-carboxylic acid hydrochloride; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

trifluoroacetic acid;