5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

Base Information

Chemical Name:5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene
CAS No.:71122-90-2
Molecular Formula:C₁₇H₁₄BrN₃O₂
Molecular Weight:372.221
Hs Code.:

Synonyms:5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

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Chemical Property of 5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

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Technology Process of 5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

There total 2 articles about 5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₄BrN₃O₂

: 71122-90-2
5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

Guidance literature:: at 20 - 25 ℃; Mechanism; Irradiation; dark decolorization time;
DOI:10.1007/BF00665585

Reference yield:

: 71122-90-2
5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

Guidance literature:: aus Dibrompropan Ie u. NH2-CH2-CH2-NH2;
DOI:10.1007/BF00471783

Reference yield: 91.0%

: 71122-90-2
5-(4-bromo-phenyl)-7-(4-nitro-phenyl)-1,4-diaza-bicyclo[4.1.0]hept-4-ene

: 98-80-6
phenylboronic acid

: 71122-92-4
1-(4-nitrophenyl)-6-(4-phenylphenyl)-1,3,4,6a-tetrahydroazireno[1,2-a]pyrazine

Guidance literature:: With sodium dodecyl-sulfate; sodium hydrogencarbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In water; toluene; butan-1-ol; for 0.0833333h; Heating;
DOI:10.1016/j.tet.2007.03.060