3,4-dihydrophenylpropionate

Base Information

Chemical Name:3,4-dihydrophenylpropionate
CAS No.:693825-21-7
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:

Synonyms:3,4-dihydrophenylpropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-dihydrophenylpropionate

Chemical Property:

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Technology Process of 3,4-dihydrophenylpropionate

There total 5 articles about 3,4-dihydrophenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 693825-14-8
ethyl 3-(cyclohexa-1,5-dienyl)propanoate

: 693825-21-7
3,4-dihydrophenylpropionate

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/jo0357667

Reference yield:

: C₉H₁₄N₂O₂

: 693825-21-7
3,4-dihydrophenylpropionate

Guidance literature:: With copper dichloride; In water; at 25 ℃; for 0.0166667h;
DOI:10.1002/anie.201609686

Reference yield:

: 63028-10-4
cyclohexa-2,4-dienyl trifluoromethanesulfonate

: 693825-21-7
3,4-dihydrophenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Zn(Cu)

1.2: 86 percent / Pd(PPh₃)4 / benzene; N,N-dimethyl-acetamide / 60 °C

2.1: 99 percent / LiOH / tetrahydrofuran; H₂O / 20 °C

With lithium hydroxide; zinc copper; In tetrahydrofuran; water; 1.2: Negishi cross-coupling;
DOI:10.1021/jo0357667