16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

Base Information

Chemical Name:16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate
CAS No.:114197-92-1
Molecular Formula:C₂₉H₃₆O₆S
Molecular Weight:512.667
Hs Code.:

Synonyms:16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

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Chemical Property of 16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

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Technology Process of 16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

There total 3 articles about 16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 114197-91-0
16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-ol

: 98-59-9
p-toluenesulfonyl chloride

: 114197-92-1
16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

Guidance literature:: With pyridine; for 24h; Ambient temperature;

Reference yield:

: 53962-63-3,53962-65-5,53962-66-6,53973-44-7
Acetic acid (8R,9S,13S,14S,16S)-16-acetoxymethyl-3-methoxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-17-yl ester

: 114197-92-1
16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 23 percent / 1 N MeONa / methanol / 1 h / Heating

2: 80 percent / pyridine / 6 h / 0 °C

3: 91 percent / pyridine / 24 h / Ambient temperature

With pyridine; sodium methylate; In methanol;

Reference yield:

: 64336-08-9
16α-hydroxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-ol

: 114197-92-1
16α-acetoxymethyl-3-methoxyestra-1,3,5(10)-trien-17β-yl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 6 h / 0 °C

2: 91 percent / pyridine / 24 h / Ambient temperature

With pyridine;