trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

Base Information

Chemical Name:trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane
CAS No.:873865-87-3
Molecular Formula:C₆₇H₉₄Si
Molecular Weight:927.569
Hs Code.:

trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9<i>H</i>,9'<i>H</i>-[2,2']bifluorenyl-7-yl)-silane

Synonyms:trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

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Technology Process of trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

There total 4 articles about trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 873866-06-9
2-iodo-9,9-dioctyl-7-phenyl-9H-fluorene

: 620624-92-2
2-(4',4',5',5'-tetramethyl-1',3',2'-dioxaborolan-2'-yl)-7-trimethylsilyl-9,9-dioctylfluorene

: 873865-87-3
trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 96h; Heating;
DOI:10.1002/chem.200500261

Reference yield:

: 873865-86-2
(9,9-dioctyl-7-phenyl-9H-fluoren-2-yl)-trimethyl-silane

: 873865-87-3
trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ICl / CH₂Cl₂ / 1 h / 0 °C

2: 91 percent / aq. NaHCO₃ / [Pd(PPh₃)4] / tetrahydrofuran / 96 h / Heating

With Iodine monochloride; sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.200500261

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 873865-87-3
trimethyl-(9,9,9',9'-tetraoctyl-7'-phenyl-9H,9'H-[2,2']bifluorenyl-7-yl)-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / aq. NaHCO₃ / [Pd(PPh₃)4] / tetrahydrofuran / 96 h / Heating

2: 98 percent / ICl / CH₂Cl₂ / 1 h / 0 °C

3: 91 percent / aq. NaHCO₃ / [Pd(PPh₃)4] / tetrahydrofuran / 96 h / Heating

With Iodine monochloride; sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; 1: Suzuki cross-coupling;
DOI:10.1002/chem.200500261