C₅₉H₆₉N₇O₁₄

Base Information

Chemical Name:C₅₉H₆₉N₇O₁₄
CAS No.:1343407-41-9
Molecular Formula:C₅₉H₆₉N₇O₁₄
Molecular Weight:1100.24
Hs Code.:

C<sub>59</sub>H<sub>69</sub>N<sub>7</sub>O<sub>14</sub>

Synonyms:C₅₉H₆₉N₇O₁₄

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Chemical Property of C₅₉H₆₉N₇O₁₄

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Technology Process of C₅₉H₆₉N₇O₁₄

There total 17 articles about C₅₉H₆₉N₇O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 55750-53-3
2,5-Dihydro-2,5-dioxo-1H-pyrrole-1-hexanoic acid

: 1343407-40-8
C₄₉H₅₈N₆O₁₁

: 1343407-41-9
C₅₉H₆₉N₇O₁₄

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In methanol; dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 1343407-39-5
C₅₃H₆₂N₆O₁₃

: 1343407-41-9
C₅₉H₆₉N₇O₁₄

Guidance literature:: Multi-step reaction with 2 steps

1: pyrrolidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / dichloromethane; methanol / 24 h / 20 °C

With pyrrolidine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane;

Reference yield:

: 1343407-31-7
C₁₅H₁₆N₂O₈

: 1343407-41-9
C₅₉H₆₉N₇O₁₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

3.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

4.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

5.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

5.2: 20 - 65 °C

6.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 6.5 h / 20 °C

8.1: pyrrolidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

9.1: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / dichloromethane; methanol / 24 h / 20 °C

With pyrrolidine; 2,6-dimethylpyridine; lithium borohydride; ethanol; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 2.1: Suzuki Coupling;