7-sulfamoyl-heptanoic acid phenylamide

Base Information

Chemical Name:7-sulfamoyl-heptanoic acid phenylamide
CAS No.:329966-86-1
Molecular Formula:C₁₃H₂₀N₂O₃S
Molecular Weight:284.379
Hs Code.:

Synonyms:7-sulfamoyl-heptanoic acid phenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-sulfamoyl-heptanoic acid phenylamide

Chemical Property:

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Technology Process of 7-sulfamoyl-heptanoic acid phenylamide

There total 4 articles about 7-sulfamoyl-heptanoic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 860315-16-8
7-sulfamoyl-heptanoic acid

: 62-53-3
aniline

: 329966-86-1
7-sulfamoyl-heptanoic acid phenylamide

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2005.04.002

Reference yield:

: 7-sulfamoylheptanoic acid ethyl ester

: 329966-86-1
7-sulfamoyl-heptanoic acid phenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / ethanol / 20 °C

2: 94 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxy-1H-benzotriazole monohydrate / dimethylformamide / 20 °C

With sodium hydroxide; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.04.002

Reference yield:

: 29823-18-5
ethyl 7-bromoheptanoate

: 329966-86-1
7-sulfamoyl-heptanoic acid phenylamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: aq. sodium sulfite / ethanol / 2 h / Heating

1.2: 93 percent / DMF; SOCl₂ / toluene / 5 h / Heating

2.1: 91 percent / aq. NH₃; 4-(dimethylamino)pyridine / tetrahydrofuran / 1 h / 20 °C

3.1: aq. NaOH / ethanol / 20 °C

4.1: 94 percent / 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxy-1H-benzotriazole monohydrate / dimethylformamide / 20 °C

With dmap; ammonium hydroxide; sodium hydroxide; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium sulfite; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.04.002