9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

Base Information

Chemical Name:9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine
CAS No.:726186-32-9
Molecular Formula:C₂₂H₂₃N₅O₇
Molecular Weight:469.454
Hs Code.:

9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N<sup>6</sup>-benzoyladenine

Synonyms:9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

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Chemical Property of 9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

Chemical Property:

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Technology Process of 9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

There total 3 articles about 9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3R,4S,5S)-4-acetoxy-5-(6-benzoylamino-purin-9-ylmethyl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yl ester

: 726186-32-9
9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

Guidance literature:: With acetic acid; at 20 ℃; for 1h;
DOI:10.1021/ja049865t

Reference yield:

: 29868-39-1
XZ-150-129-A

: 726186-32-9
9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 2 h / 0 °C

1.2: 95 percent / pyridine; aq. NaOH / ethanol / 0.5 h / 20 °C

2.1: 74 percent / pyridine / 2 h / 20 °C

3.1: pyridine / 1 h / 20 °C

4.1: 136 mg / aq. AcOH / 1 h / 20 °C

With pyridine; acetic acid;
DOI:10.1021/ja049865t

Reference yield:

: 726186-42-1
9-N-[(5'-O-(4,4'-dimethoxytrityl)-β-D-ribo-pentafuranosyl)methyl]-N⁶-benzoyladenine

: 726186-32-9
9-N-[(2',3'-O-diacetyl-β-D-ribo-pentofuranosyl)methyl]-N⁶-benzoyladenine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 20 °C

2: 136 mg / aq. AcOH / 1 h / 20 °C

With pyridine; acetic acid;
DOI:10.1021/ja049865t