Technology Process of C62H79O20P3
There total 6 articles about C62H79O20P3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate
3.1: 1H-tetrazole / dichloromethane / 3 h / 20 °C / Inert atmosphere
4.1: 1H-tetrazole / dichloromethane / 12 h / 20 °C / Inert atmosphere
4.2: -40 - 20 °C
5.1: sodium tetrahydroborate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
1H-tetrazole; sodium tetrahydroborate; hydrogen; sodium hydride;
palladium 10% on activated carbon;
In
tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate
2.1: 1H-tetrazole / dichloromethane / 3 h / 20 °C / Inert atmosphere
3.1: 1H-tetrazole / dichloromethane / 12 h / 20 °C / Inert atmosphere
3.2: -40 - 20 °C
4.1: sodium tetrahydroborate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
1H-tetrazole; sodium tetrahydroborate; hydrogen;
palladium 10% on activated carbon;
In
tetrahydrofuran; dichloromethane; ethyl acetate;