5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole

Base Information

• Chemical Name: 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole
• CAS No.: 141804-40-2
• Molecular Formula: C₂₇H₃₀N₂O₂
• Molecular Weight: 414.547

Synonyms:5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole

Chemical Property of 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole

Chemical Property:

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Technology Process of 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole

There total 8 articles about 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

5-methyl-9-hydroxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole (122490-85-1) + butyryl chloride (141-75-3) → 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole (141804-40-2)

Guidance literature:

With TEA; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1016/S0040-4020(01)88507-0

Reference yield:

5-methyl-9-formyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole (122490-84-0,143120-74-5) → 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole (141804-40-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / LiAlH₄ / diethyl ether / 2 h / -20 °C

2: 74 percent / TEA / CH₂Cl₂ / 1 h / 0 °C

With lithium aluminium tetrahydride; TEA; In diethyl ether; dichloromethane;

DOI:10.1016/S0040-4020(01)88507-0

Reference yield:

2'-phenylsulfinyl-5-methyl-12-benzyl-6,7,8,9,10,11-hexahydro-oxirano-spiro<2',9>-6,10-imino-5H-cyclooctindole (122490-83-9,122565-45-1,141847-53-2) → 5-methyl-9-butyryloxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole (141804-40-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / LiClO₄, tri-n-butylphosphine oxide / toluene / 1 h / Heating

2: 91 percent / LiAlH₄ / diethyl ether / 2 h / -20 °C

3: 74 percent / TEA / CH₂Cl₂ / 1 h / 0 °C

With lithium aluminium tetrahydride; Tributylphosphine oxide; TEA; lithium perchlorate; In diethyl ether; dichloromethane; toluene;

DOI:10.1016/S0040-4020(01)88507-0

upstream raw materials:

5-methyl-9-hydroxymethyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole

butyryl chloride

5-methyl-9-formyl-12-benzyl-6,7,10,11-tetrahydro-6,10-imino-5H-cyclooctindole

2'-phenylsulfinyl-5-methyl-12-benzyl-6,7,8,9,10,11-hexahydro-oxirano-spiro<2',9>-6,10-imino-5H-cyclooctindole

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