C₂₁H₂₃BrN₂O₃

Base Information

• Chemical Name: C₂₁H₂₃BrN₂O₃
• CAS No.: 1301177-24-1
• Molecular Formula: C₂₁H₂₃BrN₂O₃
• Molecular Weight: 431.329
• Mol file: 1301177-24-1.mol

Synonyms:C₂₁H₂₃BrN₂O₃

Chemical Property of C₂₁H₂₃BrN₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₂₃BrN₂O₃

There total 1 articles about C₂₁H₂₃BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C21H21BrN2O (1301177-22-9) → C21H23BrN2O3 (1301177-24-1)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tert-butyl alcohol;

DOI:10.1016/j.bmcl.2011.03.112

Reference yield: 100.0%

C21H23BrN2O3 (1301177-24-1) → C20H19BrN2O2 (1301177-26-3)

Guidance literature:

With sodium periodate; silica gel; In dichloromethane;

DOI:10.1016/j.bmcl.2011.03.112

Reference yield:

C21H23BrN2O3 (1301177-24-1) → C23H29BrN4O (1301177-40-1)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium periodate; silica gel / dichloromethane

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane

3: trifluoroacetic acid / dichloromethane

With sodium periodate; silica gel; sodium tris(acetoxy)borohydride; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane;

DOI:10.1016/j.bmcl.2011.02.101

upstream raw materials:

C₂₁H₂₁BrN₂O

Downstream raw materials:

C₂₃H₂₉BrN₄O

C₂₂H₂₇BrN₄O

C₂₄H₃₁BrN₄O

C₂₄H₃₁BrN₄O