{[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

Base Information

Chemical Name:{[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]
CAS No.:207226-19-5
Molecular Formula:C₄₈H₄₈O₁₀
Molecular Weight:784.903
Hs Code.:

Synonyms:{[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

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Chemical Property of {[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

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Technology Process of {[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

There total 4 articles about {[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 108059-04-7
2-allyloxy-3-hydroxybenzaldehyde

: 207226-16-2
3,3''-bis(bromomethyl)-2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl

: 207226-19-5
{[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

Guidance literature:: With potassium carbonate; In dichloromethane; acetonitrile; for 2.5h; Heating;
DOI:10.1021/jo971943q

Reference yield:

: 73229-34-2
2'-methoxy-5,5',5''-trimethyl(1,1':3',1''-terphenyl)-2,2''-diol

: 207226-19-5
{[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / trifluoroacetic acid / 3.5 h / 60 °C

2: 46 percent / K₂CO₃ / acetonitrile / 10 h / Heating

3: NaBH₄ / methanol; tetrahydrofuran / 3 h / Ambient temperature

4: PBr₃ / toluene / 0 °C

5: 47 percent / K₂CO₃ / acetonitrile; CH₂Cl₂ / 2.5 h / Heating

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile; trifluoroacetic acid;
DOI:10.1021/jo971943q

Reference yield:

: 207226-13-9
3,3''-[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl]dimethanol

: 207226-19-5
{[2,2''-bis((2,1-ethanediyloxy)oxy)-2'-methoxy-5,5',5''-trimethyl[1,1':3',1'']terphenyl-3,3''-diyl]bis(methyleneoxy)}bis[2-(2-propenyloxy)benzaldehyde]

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / toluene / 0 °C

2: 47 percent / K₂CO₃ / acetonitrile; CH₂Cl₂ / 2.5 h / Heating

With phosphorus tribromide; potassium carbonate; In dichloromethane; toluene; acetonitrile;
DOI:10.1021/jo971943q