2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

Base Information

Chemical Name:2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat
CAS No.:110797-43-8
Molecular Formula:C₄₀H₃₆Cl₃NO₁₀
Molecular Weight:797.086
Hs Code.:

Synonyms:2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

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Chemical Property of 2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

Chemical Property:

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Technology Process of 2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

There total 7 articles about 2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 110797-42-7
2,3,4,6-Tetra-p-toluyl-α-D-galactopyranose

: 545-06-2
trichloroacetonitrile

: 110797-43-8
2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

Guidance literature:: With sodium hydride; In dichloromethane; for 1h;

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 110797-43-8
2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / pyridine / CH₂Cl₂ / 18 h / Ambient temperature

2: 78 percent / 65percent HClO₄ / 3 h

3: 57 percent / NaH / CH₂Cl₂ / 1 h

With pyridine; perchloric acid; sodium hydride; In dichloromethane;

Reference yield:

: 110797-45-0
1,2,3,4,6-Penta-O-p-toluyl-α-D-galactopyranosid

: 110797-43-8
2,3,4,6-Tetra-O-p-toluyl-α/β-D-galactopyranosyl-trichloracetimidat

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 65percent HClO₄ / 3 h

2: 57 percent / NaH / CH₂Cl₂ / 1 h

With perchloric acid; sodium hydride; In dichloromethane;