diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

Base Information

Chemical Name:diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether
CAS No.:374928-87-7
Molecular Formula:C₂₈H₃₅F₁₇OSi
Molecular Weight:738.644
Hs Code.:

Synonyms:diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

There total 3 articles about diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2430-16-2
6-phenyl-1-hexanol

: 356056-15-0
diisopropyl(3’,3’,4’,4’,5’,5’,6’,6’,7’,7’,8’,8’,9’,9’,10’,10’-heptadecafluorodecyl)silane

: 374928-87-7
diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

Guidance literature:: diisopropyl(3’,3’,4’,4’,5’,5’,6’,6’,7’,7’,8’,8’,9’,9’,10’,10’-heptadecafluorodecyl)silane; With bromine; In diethyl ether; at 0 ℃;

6-phenyl-1-hexanol; With dmap; triethylamine; In dichloromethane; at 0 ℃; Further stages.;
DOI:10.1021/ja011716c

Reference yield:

: 2043-53-0,71215-70-8
2-(n-perfluorooctyl)ethyl iodide

: 374928-87-7
diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / t-BuLi / diethyl ether; hexane / -78 - 20 °C

2.1: Br₂ / diethyl ether / 0 °C

2.2: 4-dimethylaminopyridine; triethylamine / CH₂Cl₂ / 0 °C

With bromine; tert.-butyl lithium; In diethyl ether; hexane;
DOI:10.1021/ja011716c

Reference yield:

: 2227-29-4
chlorodiisopropylsilane

: 374928-87-7
diisopropyl-1H,1H,2H,2H-perfluorodecylsilyl 6-phenylhexyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / t-BuLi / diethyl ether; hexane / -78 - 20 °C

2.1: Br₂ / diethyl ether / 0 °C

2.2: 4-dimethylaminopyridine; triethylamine / CH₂Cl₂ / 0 °C

With bromine; tert.-butyl lithium; In diethyl ether; hexane;
DOI:10.1021/ja011716c