Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester

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Chemical Name:Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester
CAS No.:1026926-07-7
Molecular Formula:C₁₃H₁₅NO₄
Molecular Weight:249.266
Hs Code.:

Synonyms:Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester

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Chemical Property of Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester

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Technology Process of Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester

There total 1 articles about Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26054-46-6
(-)-(1S,5R)-2-oxabicyclo[3.3.0]oct-6-en-3-one

: 1026926-07-7
Carbonic acid (3aR,4S,6aR)-(hexahydro-cyclopenta[b]furan-4-yl) ester pyridin-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 96.4 percent / LiAlH₄ / tetrahydrofuran / 4 h / Ambient temperature

2: 86 percent / aq. NaHCO₃, KI, I₂ / CH₂Cl₂ / Ambient temperature

3: 81 percent / n-Bu₃SnH, AIBN / dioxane / Heating

4: Et₃N / CH₂Cl₂ / 12 h / 23 °C

With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); iodine; tri-n-butyl-tin hydride; sodium hydrogencarbonate; triethylamine; potassium iodide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/jm960128k