15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

Base Information

Chemical Name:15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin
CAS No.:1443667-02-4
Molecular Formula:C₄₆H₂₃F₁₀N₅O₂
Molecular Weight:867.705
Hs Code.:

Synonyms:15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

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Chemical Property of 15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

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Technology Process of 15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

There total 5 articles about 15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1443667-01-3
15-(4-carbomethoxyphenyl)-5-(N-tert-butoxycarbonyl-4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

: 1443667-02-4
15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

Guidance literature:: In dichloromethane; trifluoroacetic acid; at 20 ℃; for 0.666667h;
DOI:10.1039/c3dt50711d

Reference yield:

: 167482-91-9
5-(pentafluorophenyl)dipyrromethane

: 1443667-02-4
15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; trifluoroacetic acid / 1.67 h / 20 °C

2: trifluoroacetic acid; hydrogenchloride / 60 °C / liquid HCl

3: diphenyl phosphoryl azide / trifluoroacetic acid / 48 h / 80 °C

4: dichloromethane; trifluoroacetic acid / 0.67 h / 20 °C

With diphenyl phosphoryl azide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In hydrogenchloride; dichloromethane; trifluoroacetic acid;
DOI:10.1039/c3dt50711d

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 1443667-02-4
15-(4-carbomethoxyphenyl)-5-(4-aminophenyl)-10,20-bis(2,3,4,5,6-pentafluorophenyl) porphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; trifluoroacetic acid / 1.67 h / 20 °C

2: trifluoroacetic acid; hydrogenchloride / 60 °C / liquid HCl

3: diphenyl phosphoryl azide / trifluoroacetic acid / 48 h / 80 °C

4: dichloromethane; trifluoroacetic acid / 0.67 h / 20 °C

With diphenyl phosphoryl azide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In hydrogenchloride; dichloromethane; trifluoroacetic acid;
DOI:10.1039/c3dt50711d