Bis(N-t-butyl-N'-ethylpropanimidamidato)cobalt(II), min. 98% (99.99%-Co) PURATREM

Base Information

• Chemical Name: Bis(N-t-butyl-N'-ethylpropanimidamidato)cobalt(II), min. 98% (99.99%-Co) PURATREM
• CAS No.: 1011477-51-2
• Molecular Formula: C₁₈H₃₈CoN₄
• Molecular Weight: 369.52
• Mol file: 1011477-51-2.mol

Synonyms:bis(N-tert-butyl-N'-ethylpropionamidinato) cobalt(II)

Chemical Property of Bis(N-t-butyl-N'-ethylpropanimidamidato)cobalt(II), min. 98% (99.99%-Co) PURATREM

Chemical Property:

• Melting Point: -17 °C
• Sensitive.: air sensitive, moisture sensitiv

Purity/Quality:

98% ^*data from raw suppliers

Bis(N-t-butyl-N'-ethylpropanimidamidato)cobalt(II), min. 98% (99.99%-Co) PURATREM ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Volatile cobalt complex for the atomic layer deposition of cobalt metal. Volatile Cobalt precursor for ALD/CVD

Technology Process of Bis(N-t-butyl-N'-ethylpropanimidamidato)cobalt(II), min. 98% (99.99%-Co) PURATREM

There total 1 articles about Bis(N-t-butyl-N'-ethylpropanimidamidato)cobalt(II), min. 98% (99.99%-Co) PURATREM which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butyl-N'-ethylcarbodiimide (1433-27-8) + ethyllithium (811-49-4) + cobalt(II) chloride (7646-79-9,14543-09-0,16413-89-1) → bis(N-tert-butyl-N'-ethylpropionamidinato) cobalt(II) (1011477-51-2)

Guidance literature:

In tetrahydrofuran; hexane; (under N2, Schlenk); soln. of LiCH2CH3 in hexane added dropwise to soln.of ligand in THF at -78°C, warmed to room temp., stirred for 4 h , soln. of CoCl2 in THF added at room temp., stirred for 12 h; volatiles removed under reduced pressure, ppt. extd. with pentane, filtered, pentane removed under reduced pressure, distilled at 90°C, 30 mTorr; elem. anal.;

DOI:10.1039/b800712h

Reference yield:

bis(N-tert-butyl-N'-ethylpropionamidinato) cobalt(II) (1011477-51-2) → cobalt (7440-48-4)

Guidance literature:

With ammonia; hydrogen; at 150 - 200 ℃;

upstream raw materials:

N-tert-butyl-N'-ethylcarbodiimide

ethyllithium

cobalt(II) chloride

Downstream raw materials:

cobalt

Refernces