1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane

Base Information

Chemical Name:1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane
CAS No.:1356031-32-7
Molecular Formula:C₅₂H₄₆N₄O₂
Molecular Weight:758.963
Hs Code.:

Synonyms:1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane

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Chemical Property of 1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane

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Technology Process of 1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane

There total 2 articles about 1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1173177-78-0
C₂₀H₁₆N₆O₂

: 678556-45-1
1-(4-methylbenzyl)-1H-indole

: 1356031-32-7
1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane

Guidance literature:: With dirhodium tetraacetate; In dichloromethane; at 25 ℃; for 0.25h; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.073

Reference yield:

: 3265-29-0
3-diazo-indolin-2-one

: 1356031-32-7
1,4-bis[(1'-(4-methylbenzyl)-1,3-dihydro-1'H-[3,3']biindolyl-2-on)-1-yl]butane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere

2: dirhodium tetraacetate / dichloromethane / 0.25 h / 25 °C / Inert atmosphere

With dirhodium tetraacetate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.11.073