13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

Base Information

Chemical Name:13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane
CAS No.:1418227-03-8
Molecular Formula:C₃₀H₃₂N₂O₆
Molecular Weight:516.594
Hs Code.:

Synonyms:13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

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Chemical Property of 13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

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Technology Process of 13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

There total 3 articles about 13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1418227-02-7
9-(5-chloro-2-nitrobenzylidene)-9H-fluorene

: 66943-05-3
1,4,7,10-tetraoxa-15-azacyclopentadecane

: 1418227-03-8
13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

Guidance literature:: With 1,10-Phenanthroline; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1002/cjoc.201200047

Reference yield:

: 587-04-2
m-Chlorobenzaldehyde

: 1418227-03-8
13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid

2: chloroform / 3 h / Reflux

3: 1,10-Phenanthroline / N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 80 °C / Inert atmosphere

With 1,10-Phenanthroline; nitric acid; In N,N,N,N,N,N-hexamethylphosphoric triamide; chloroform;
DOI:10.1002/cjoc.201200047

Reference yield:

: 6628-86-0
5-chloro-2-nitrobenzaldehyde

: 1418227-03-8
13-((2-(9H-fluoren-9-ylidene)methyl)-4-nitrophenyl)-1,4,7,10-tetraoxa-3-azacyclopentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 3 h / Reflux

2: 1,10-Phenanthroline / N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 80 °C / Inert atmosphere

With 1,10-Phenanthroline; In N,N,N,N,N,N-hexamethylphosphoric triamide; chloroform;
DOI:10.1002/cjoc.201200047