C₂₂H₂₀ClN₃O₄S₂

Base Information

Chemical Name:C₂₂H₂₀ClN₃O₄S₂
CAS No.:1613712-14-3
Molecular Formula:C₂₂H₂₀ClN₃O₄S₂
Molecular Weight:490.003
Hs Code.:

C<sub>22</sub>H<sub>20</sub>ClN<sub>3</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₂H₂₀ClN₃O₄S₂

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Chemical Property of C₂₂H₂₀ClN₃O₄S₂

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Technology Process of C₂₂H₂₀ClN₃O₄S₂

There total 3 articles about C₂₂H₂₀ClN₃O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55052-28-3
4-chloro-7-azaindole

: 1613712-14-3
C₂₂H₂₀ClN₃O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; N-chloro-succinimide / 4 h / 0 - 20 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 0 °C / Inert atmosphere

3: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / acetonitrile / 4.25 h / 85 °C / Inert atmosphere; Sealed tube

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-chloro-succinimide; sodium hydride; caesium carbonate; acetic acid; In N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 869335-20-6
4-chloro-3-iodo-1-[(4-methylphenyl)sulfonyl]-1H-pyrrolo[2,3-b]pyridine

: 178432-25-2
(2-(N,N-dimethylsulfamoyl)phenyl)boronic acid

: 1613712-14-3
C₂₂H₂₀ClN₃O₄S₂

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In acetonitrile; at 85 ℃; for 4.25h; Inert atmosphere; Sealed tube;

Reference yield:

: 869335-73-9
4-chloro-3-iodo-1H-pyrrolo[2,3-b]pyridine

: 1613712-14-3
C₂₂H₂₀ClN₃O₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 6 h / 0 °C / Inert atmosphere

2: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / acetonitrile / 4.25 h / 85 °C / Inert atmosphere; Sealed tube

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydride; caesium carbonate; In N,N-dimethyl-formamide; acetonitrile; mineral oil;