3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

Base Information

Chemical Name:3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione
CAS No.:1017238-99-1
Molecular Formula:C₂₃H₁₉N₃O₅
Molecular Weight:417.421
Hs Code.:

Synonyms:3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

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Chemical Property of 3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

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Technology Process of 3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

There total 12 articles about 3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 85-44-9
phthalic anhydride

: 99-61-6
3-nitro-benzaldehyde

: 126-81-8
dimedone

: 1017238-99-1
3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

Guidance literature:: With hydrazine hydrate; N,N,N',N'-tetramethylguanidinium acetate; In neat (no solvent); at 80 ℃; for 0.166667h; Green chemistry;
DOI:10.1039/c4ra03514c

Reference yield: 98.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 99-61-6
3-nitro-benzaldehyde

: 126-81-8
dimedone

: 1017238-99-1
3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

Guidance literature:: With phospho sulphonic acid; In neat (no solvent); at 100 ℃; for 0.0833333h;
DOI:10.2298/JSC120508088K

Reference yield: 94.0%

: 85-44-9
phthalic anhydride

: 79785-97-0
hydrazine hydrate

: 99-61-6
3-nitro-benzaldehyde

: 126-81-8
dimedone

: 1017238-99-1
3,4-dihydro-3,3-dimethyl-13-(3-nitrophenyl)-2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione

Guidance literature:: With 1,4-dimethyl-1-(4-sulphobutyl)piperazinium hydrogen sulphate; at 80 ℃; for 0.0833333h; Green chemistry;
DOI:10.1007/s11164-014-1736-0