1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl

Base Information

• Chemical Name: 1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl
• CAS No.: 335629-05-5
• Molecular Formula: C₁₄₀H₁₉₉N₇O₄₄S₂
• Molecular Weight: 2748.27

Synonyms:1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl

Chemical Property of 1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl

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Technology Process of 1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl

There total 1 articles about 1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

4,4,5,5-tetramethyl-2-(4-methylsulfanylphenyl)-[1,3,2]-dioxaborolane (190788-58-0) + 64,14-diiodo-63,52,43,32,23,13-hexa(18-azacrown-6-N-carbonylmethoxy)-p-sexiphenyl (256387-79-8) + N-(t-Boc)-2-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylsulfanyl]ethylamine (335629-02-2) → 84,14-dimethylsulfanyl-73,62,53,42,33,22-hexa(18-azacrown-6-N-carbonylmethoxy)-p-octiphenyl (256387-82-3) + 14-2'-t-Boc-aminoethylthio-84-methylthio-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl (335629-05-5) + C146H210N8O46S2

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In ethanol; toluene; at 80 ℃; for 21h;

DOI:10.1021/ja003141+

Reference yield: 90.0%

trifluoroacetic acid (76-05-1) + 14-2'-t-Boc-aminoethylthio-84-methylthio-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl (335629-05-5) → 14-2'-aminoethylthio-84-methylthio-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl, trifluoroacetic acid

Guidance literature:

In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1021/ja003141+

Reference yield: 25.0%

14-2'-t-Boc-aminoethylthio-84-methylthio-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl (335629-05-5) → 14-2'-t-Boc-aminoethylsulfonyl-84-methylthio-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl + 14-2'-t-Boc-aminoethylthio-84-methylsulfonyl-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl + 14-2'-t-Boc-aminoethylsulfonyl-84-methylsulfonyl-73,62,53,42,33,22-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl

Guidance literature:

1⁴-2'-t-Boc-aminoethylthio-8⁴-methylthio-7³,6²,5³,4²,3³,2²-hexa(18-aza-6-N-carbonylmethoxy)-p-octiphenyl; With 3-chloro-benzenecarboperoxoic acid; In acetone; at 0 ℃; for 2h;

With potassium permanganate; magnesium sulfate; In acetone; at 20 ℃; for 1h;

With trifluoroacetic anhydride; sodium iodide; In acetone; at 0 ℃; for 0.166667h; Further stages.;

DOI:10.1021/ja003141+

upstream raw materials:

4,4,5,5-tetramethyl-2-(4-methylsulfanylphenyl)-[1,3,2]-dioxaborolane

6⁴,1⁴-diiodo-6³,5²,4³,3²,2³,1³-hexa(18-azacrown-6-N-carbonylmethoxy)-p-sexiphenyl

N-(t-Boc)-2-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenylsulfanyl]ethylamine

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