(2E)-3-(2-methoxyphenyl)prop-2-enoyl azide

Base Information

Chemical Name:(2E)-3-(2-methoxyphenyl)prop-2-enoyl azide
CAS No.:118652-95-2
Molecular Formula:C₁₀H₉N₃O₂
Molecular Weight:203.2
Hs Code.:
DSSTox Substance ID:DTXSID001265318

Synonyms:118652-95-2;(2E)-3-(2-methoxyphenyl)prop-2-enoyl azide;SCHEMBL16470964;DTXSID001265318;STL072933;AKOS005655927;(2E)-3-(2-Methoxyphenyl)-2-propenoyl azide

Suppliers and Price of (2E)-3-(2-methoxyphenyl)prop-2-enoyl azide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of (2E)-3-(2-methoxyphenyl)prop-2-enoyl azide

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:203.069476538
Heavy Atom Count:15
Complexity:295

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=CC=C1C=CC(=O)N=[N+]=[N-]
Isomeric SMILES:COC1=CC=CC=C1/C=C/C(=O)N=[N+]=[N-]

Technology Process of (2E)-3-(2-methoxyphenyl)prop-2-enoyl azide

There total 3 articles about (2E)-3-(2-methoxyphenyl)prop-2-enoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118652-93-0
o-methoxycinnamoyl chloride

: 118652-95-2
3-(2-methoxy-phenyl)-acryloyl azide

Guidance literature:: With sodium azide; In water; acetone; at 20 ℃; for 3h;

Reference yield:

: C₁₃H₁₄O₅

: 118652-95-2
3-(2-methoxy-phenyl)-acryloyl azide

Guidance literature:: With sodium azide; In water; acetone; at 0 ℃; for 1h;
DOI:10.1016/j.bmcl.2012.11.069

Reference yield:

: 1011-54-7
2-methoxycinnamic acid

: 118652-95-2
3-(2-methoxy-phenyl)-acryloyl azide

Guidance literature:: With sodium azide; chloroformic acid ethyl ester; triethylamine; Multistep reaction; 1.) ethyl chloroformate, acetone, triethylamine, 0 deg C, 30 min 2.) sodium azide, water, 15 deg C, 1 h;