Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester
CAS No.:188444-67-9
Molecular Formula:C₃₂H₃₄N₂O₁₄S
Molecular Weight:702.693
Hs Code.:

Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

Synonyms:Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

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Chemical Property of Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

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Technology Process of Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

There total 1 articles about Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose

: 188444-66-8
4-nitro-N-[2-(2-naphthyloxy)ethyl]benzenesulfonamide

: 188444-67-9
Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -80 - 20 ℃; for 19h;
DOI:10.1002/ejoc.200600132

Reference yield: 95.0%

: 188444-67-9
Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

: 188444-68-0
N-[2-(Naphthalen-2-yloxy)-ethyl]-4-nitro-N-((2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yl)-benzenesulfonamide

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 24h;
DOI:10.1002/ejoc.200600132

Reference yield:

: 188444-67-9
Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[[2-(naphthalen-2-yloxy)-ethyl]-(4-nitro-benzenesulfonyl)-amino]-tetrahydro-pyran-3-yl ester

: 188480-51-5
SCH-54292

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / methanol / 24 h / 20 °C

2: 93 percent / hydrazine hydrate / Pd/C / tetrahydrofuran / 0.75 h / 0 °C

With potassium carbonate; hydrazine hydrate; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1002/ejoc.200600132