3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

Base Information

• Chemical Name: 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol
• CAS No.: 1310450-10-2
• Molecular Formula: C₂₉H₃₄O₆
• Molecular Weight: 478.585

Synonyms:3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

Chemical Property of 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

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Technology Process of 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol

There total 2 articles about 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

C50H53NO6 (1310450-12-4) → 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol (1310450-10-2)

Guidance literature:

In methanol; acetonitrile; at 20 - 30 ℃; for 4.5h; Irradiation;

DOI:10.1021/jo200692c

Reference yield: 81.0%

allyl 2,3,4-tri-O-benzyl-α-D-xylopyranoside (196859-38-8) → 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol (1310450-10-2)

Guidance literature:

allyl 2,3,4-tri-O-benzyl-α-D-xylopyranoside; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/jo200692c

Reference yield: 91.0%

3-(dimethylamino)-α,α-diphenylbenzenemethanol 1-acetate (1220688-48-1) + 3-(((2S,3R,4S,5R)-3,4,5-tris(benzyloxy)tetrahydro-2H-pyran-2-yl)oxy)propan-1-ol (1310450-10-2) → C50H53NO6 (1310450-12-4)

Guidance literature:

In toluene; at 120 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo200692c

upstream raw materials:

C₅₀H₅₃NO₆

allyl 2,3,4-tri-O-benzyl-α-D-xylopyranoside

Downstream raw materials:

C₅₀H₅₃NO₆

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