C₂₉H₃₂Cl₆N₆O₅SSi

Base Information

Chemical Name:C₂₉H₃₂Cl₆N₆O₅SSi
CAS No.:1061574-23-9
Molecular Formula:C₂₉H₃₂Cl₆N₆O₅SSi
Molecular Weight:817.48
Hs Code.:

C<sub>29</sub>H<sub>32</sub>Cl<sub>6</sub>N<sub>6</sub>O<sub>5</sub>SSi

Synonyms:C₂₉H₃₂Cl₆N₆O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₂Cl₆N₆O₅SSi

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Technology Process of C₂₉H₃₂Cl₆N₆O₅SSi

There total 9 articles about C₂₉H₃₂Cl₆N₆O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1061574-04-6
C₃₁H₃₄Cl₆N₆O₇SSi

: 1061574-23-9
C₂₉H₃₂Cl₆N₆O₅SSi

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃; for 1.5h;

Reference yield: 83.0%

: C₃₁H₃₄Cl₆N₆O₇SSi

: 1061574-23-9
C₂₉H₃₂Cl₆N₆O₅SSi

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jacs.6b02343

Reference yield:

: 1061574-16-0
C₂₈H₃₃Cl₃N₄O₅S₂Si

: 1061574-23-9
C₂₉H₃₂Cl₆N₆O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: 2,4,6-tri-tert-butylpyrimidine / dichloromethane / 29 h / 37 °C / Inert atmosphere; Sealed tube

2: ammonia / methanol / 24 h / 70 °C / Inert atmosphere; Sealed tube

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -20 °C / Inert atmosphere

4: bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; magnesium oxide / dichloromethane / 2.5 h / 42 °C / Inert atmosphere; Sealed tube

5: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 1.5 h / -78 - 20 °C / Inert atmosphere

With triethylsilane; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; boron trifluoride diethyl etherate; ammonia; magnesium oxide; N-ethyl-N,N-diisopropylamine; 2,4,6-tri-tert-butylpyrimidine; In methanol; dichloromethane;
DOI:10.1021/jacs.6b02343