2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

Base Information

Chemical Name:2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside
CAS No.:96530-50-6
Molecular Formula:C₄₀H₃₈O₉
Molecular Weight:662.736
Hs Code.:

Synonyms:2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

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Chemical Property of 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

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Technology Process of 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

There total 2 articles about 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.5%

: 96530-47-1
2-O-benzyl-4,6-O-benzylidene-3-O-trifluoromethylsulfonyl-α-D-altropyranosyl 2-O-benzyl-4,6-O-benzylidene-3-O-trifluoromethylsulfonyl-α-D-altropyranoside

: 96530-50-6
2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

: 3-azido-2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-mannopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

: 3-azido-2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-mannopyranosyl 3-azido-2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-mannopyranoside

Guidance literature:: With sodium azide; tetra(n-butyl)ammonium hydrogensulfate; In water; benzene; for 120h; Heating;
DOI:10.1139/v85-072

Reference yield:

: 90593-18-3
2-O-benzyl-4,6-O-benzylidene-α-D-altropyranosyl 2-O-benzyl-4,6-O-benzylidene-α-D-altropyranoside

: 96530-50-6
2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranosyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-threo-hex-3-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94.4 percent / pyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

2: 1.5 percent / sodium azide / tetrabutylammonium hydrogen sulfate / benzene; H₂O / 120 h / Heating

With pyridine; sodium azide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; water; benzene;
DOI:10.1139/v85-072