Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester

Base Information

• Chemical Name: Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester
• CAS No.: 192518-28-8
• Molecular Formula: C₇₉H₁₂₆N₈O₈
• Molecular Weight: 1315.92

Synonyms:Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester

Chemical Property of Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester

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Technology Process of Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester

There total 1 articles about Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4,8,12-Tetraazacyclopentadecan (15439-16-4) + Toluene-4-sulfonic acid 5-(benzyl-tert-butoxycarbonyl-amino)-pentyl ester (204773-56-8) → Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester (192518-28-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃;

DOI:10.1016/S0960-894X(97)00222-9

Reference yield: 61.0%

Toluene-4-sulfonic acid 5-(benzyl-tert-butoxycarbonyl-amino)-pentyl ester (204773-56-8) + Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester (192518-28-8) → C96H152N9O10(1+)*C7H7O3S(1-)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 110 ℃; for 48h;

DOI:10.1016/S0960-894X(97)00222-9

Reference yield:

Benzyl-(5-{4,8,12-tris-[5-(benzyl-tert-butoxycarbonyl-amino)-pentyl]-1,4,8,12-tetraaza-cyclopentadec-1-yl}-pentyl)-carbamic acid tert-butyl ester (192518-28-8) → Benzyl-{5-[4,8,12-tris-(5-benzylamino-pentyl)-1,4,8,12-tetraaza-cyclopentadec-1-yl]-pentyl}-amine

Guidance literature:

With hydrogenchloride; In methanol; Ambient temperature;

DOI:10.1016/S0960-894X(97)00222-9

upstream raw materials:

1,4,8,12-Tetraazacyclopentadecan

Toluene-4-sulfonic acid 5-(benzyl-tert-butoxycarbonyl-amino)-pentyl ester

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