Technology Process of C39H44N2O8
There total 10 articles about C39H44N2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1021/ja077853c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ammonium chloride; zinc / ethanol; water / 90 °C
2: sodium hydrogencarbonate / 1,4-dioxane; water / 4 h / 0 °C
3: toluene-4-sulfonic acid / methanol / 48 h / 20 °C
4: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
With
sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane; toluene-4-sulfonic acid; zinc;
In
1,4-dioxane; methanol; ethanol; dichloromethane; water;
4: Dess-Martin oxidation;
DOI:10.1021/jo200553g
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: magnesium sulfate / dichloromethane / 4 h / 20 °C
2.1: iodine; magnesium; ethylene dibromide / tetrahydrofuran / Reflux
2.2: 5 h / -50 °C
3.1: ammonium chloride; zinc / ethanol; water / 90 °C
4.1: sodium hydrogencarbonate / 1,4-dioxane; water / 4 h / 0 °C
5.1: toluene-4-sulfonic acid / methanol / 48 h / 20 °C
6.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
With
iodine; sodium hydrogencarbonate; magnesium sulfate; ammonium chloride; Dess-Martin periodane; toluene-4-sulfonic acid; magnesium; ethylene dibromide; zinc;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water;
6.1: Dess-Martin oxidation;
DOI:10.1021/jo200553g
