C₂₃H₂₉N₃O₆S

Base Information

Chemical Name:C₂₃H₂₉N₃O₆S
CAS No.:1449016-67-4
Molecular Formula:C₂₃H₂₉N₃O₆S
Molecular Weight:475.566
Hs Code.:

C<sub>23</sub>H<sub>29</sub>N<sub>3</sub>O<sub>6</sub>S

Synonyms:C₂₃H₂₉N₃O₆S

Suppliers and Price of C₂₃H₂₉N₃O₆S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₂₉N₃O₆S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₂₉N₃O₆S

There total 6 articles about C₂₃H₂₉N₃O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1449016-66-3
C₂₃H₂₉N₃O₆S

: 1449016-67-4
C₂₃H₂₉N₃O₆S

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; ethene; In dichloromethane; at -10 - 45 ℃; for 24h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/ejoc.201201516

Reference yield:

: 60410-16-4
(1R,4S)-4-hydroxy-2-cyclopentene-1-yl acetate

: 1449016-67-4
C₂₃H₂₉N₃O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 0 - 20 °C

2.1: potassium carbonate; thiophenol / tetrahydrofuran; N,N-dimethyl-formamide / 3.5 h / 20 - 70 °C

2.2: 12 h / 60 °C

2.3: 12 h / 20 °C

3.1: potassium hydride; dibenzo-18-crown-6 / tetrahydrofuran / 20 °C

4.1: n-butyllithium / tetrahydrofuran / 17.5 h / -100 - -60 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 0 °C

6.1: Hoveyda-Grubbs catalyst second generation; ethene / dichloromethane / 24 h / -10 - 45 °C / 760.05 Torr / Inert atmosphere

With dibenzo-18-crown-6; n-butyllithium; Hoveyda-Grubbs catalyst second generation; ethene; di-isopropyl azodicarboxylate; potassium hydride; potassium carbonate; thiophenol; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: |Fukuyama Coupling / 3.1: |Williamson Ether Synthesis / 4.1: |Wittig Rearrangement / 5.1: |Fukuyama Coupling;
DOI:10.1002/ejoc.201201516

Reference yield:

: 1449016-83-4
C₁₆H₁₈N₂O₆S

: 1449016-67-4
C₂₃H₂₉N₃O₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; thiophenol / tetrahydrofuran; N,N-dimethyl-formamide / 3.5 h / 20 - 70 °C

1.2: 12 h / 60 °C

1.3: 12 h / 20 °C

2.1: potassium hydride; dibenzo-18-crown-6 / tetrahydrofuran / 20 °C

3.1: n-butyllithium / tetrahydrofuran / 17.5 h / -100 - -60 °C

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 0 °C

5.1: Hoveyda-Grubbs catalyst second generation; ethene / dichloromethane / 24 h / -10 - 45 °C / 760.05 Torr / Inert atmosphere

With dibenzo-18-crown-6; n-butyllithium; Hoveyda-Grubbs catalyst second generation; ethene; di-isopropyl azodicarboxylate; potassium hydride; potassium carbonate; thiophenol; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2.1: |Williamson Ether Synthesis / 3.1: |Wittig Rearrangement / 4.1: |Fukuyama Coupling;
DOI:10.1002/ejoc.201201516