2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone

Base Information

• Chemical Name: 2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone
• CAS No.: 924891-96-3
• Molecular Formula: C₂₇H₁₇NO₆
• Molecular Weight: 451.435

Synonyms:2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone

Chemical Property of 2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone

Chemical Property:

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Technology Process of 2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone

There total 1 articles about 2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4'-(1,3-dioxo-1,3-dihydro-2H-inden-2-ylidene)spiro[indene-2,3'-oxetane]-1,2',3-trione + p-toluidine (106-49-0,12221-03-3) → (2E,3E)-2-{hydroxy[(4-methylphenyl)amino]methylene}-3-[(4-methylphenyl)imino]indan-1-one + 2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone (924891-96-3)

Guidance literature:

In dichloromethane;

DOI:10.1021/jo061879p

Reference yield: 80.0%

2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone (924891-96-3) + N-methylaniline (100-61-8) → 2-[1-Hydroxy-1-(methyl-phenyl-amino)-meth-(E)-ylidene]-3-[(E)-p-tolylimino]-indan-1-one

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/jo061879p

Reference yield:

2-Hydroxy-3-{hydroxy-[1-oxo-3-[(E)-p-tolylimino]-indan-(2Z)-ylidene]-methoxy}-[1,4]naphthoquinone (924891-96-3) + p-toluidine (106-49-0,12221-03-3) → (2E,3E)-2-{hydroxy[(4-methylphenyl)amino]methylene}-3-[(4-methylphenyl)imino]indan-1-one

Guidance literature:

In dichloromethane;

DOI:10.1021/jo061879p

upstream raw materials:

p-toluidine

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