tert-butyl-(-)-menthyltin(IV) dibromide

Base Information

Chemical Name:tert-butyl-(-)-menthyltin(IV) dibromide
CAS No.:142189-15-9
Molecular Formula:C₁₄H₂₈Br₂Sn
Molecular Weight:474.894
Hs Code.:

Synonyms:tert-butyl-(-)-menthyltin(IV) dibromide

Suppliers and Price of tert-butyl-(-)-menthyltin(IV) dibromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tert-butyl-(-)-menthyltin(IV) dibromide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl-(-)-menthyltin(IV) dibromide

There total 1 articles about tert-butyl-(-)-menthyltin(IV) dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 125002-48-4
tert-butyl-(-)-menthyldimethyltin(IV)

: 142189-15-9
tert-butyl-(-)-menthyltin(IV) dibromide

Guidance literature:: With Br₂; In methanol; under Ar, the Sn complex treated with Br2 (0°C, under exclusion of light), reacted (4 days); solvent removed (vac.), residue distilled, filtered, fractionated distillation; elem. anal.;
DOI:10.1021/om00044a019

Reference yield: 60.0%

: 142189-15-9
tert-butyl-(-)-menthyltin(IV) dibromide

: 8-dimethylamino-1-naphthyllithium*(diethyl ether)

: 142189-17-1
tert-butyl-8-(diamino)naphthyl-(-)-menthyltin(IV) bromide

Guidance literature:: In diethyl ether; under Ar, C10H6(NMe2)Li*Et2O soln. added to a stirred soln. of the Sn complex (4 h, 10°C), stirred (50 h, room temp.); solvent removed (vac.), residue extracted (hot benzene), concentrated, crystn. (toluene/pentane, -30°C), recrystn. (pentane); elem. anal.;
DOI:10.1021/om00044a019