4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

Base Information

Chemical Name:4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide
CAS No.:947263-60-7
Molecular Formula:C₂₃H₃₆IN₃O₅
Molecular Weight:561.46
Hs Code.:

Synonyms:4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

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Chemical Property of 4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

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Technology Process of 4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

There total 9 articles about 4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947263-46-9
4-(N-tert-butoxycarbonyl-N-butylamino)butyronitrile

: 947263-60-7
4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 1 h / 0 °C

2: 1.2 g / triethylamine / tetrahydrofuran / 2 h

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm0701627

Reference yield:

: 4-(butylamino)butyronitrile

: 947263-60-7
4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 15 h / 20 °C

2: LiAlH₄ / diethyl ether / 1 h / 0 °C

3: 1.2 g / triethylamine / tetrahydrofuran / 2 h

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/jm0701627

Reference yield:

: 27492-84-8
Methyl 4-amino-2-methoxybenzoate

: 947263-60-7
4-acetamido-N-(4-(N-tert-butoxycarbonyl-N-butylamino)butyl)-5-iodo-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / ethanol / 2 h / 50 °C

2: 77 percent / iodine monochloride; acetic acid / 6 h / 50 °C

3: KOH / methanol; H₂O / 2 h / Heating

4: 1.5 g / acetic acid / 2 h / 50 °C

5: thionyl chloride / tetrahydrofuran / 2 h / Heating

6: 1.2 g / triethylamine / tetrahydrofuran / 2 h

With potassium hydroxide; thionyl chloride; Iodine monochloride; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/jm0701627