C₃₂H₄₁ClN₆O₄Si

Base Information

Chemical Name:C₃₂H₄₁ClN₆O₄Si
CAS No.:1364718-73-9
Molecular Formula:C₃₂H₄₁ClN₆O₄Si
Molecular Weight:637.254
Hs Code.:

C<sub>32</sub>H<sub>41</sub>ClN<sub>6</sub>O<sub>4</sub>Si

Synonyms:C₃₂H₄₁ClN₆O₄Si

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Chemical Property of C₃₂H₄₁ClN₆O₄Si

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Technology Process of C₃₂H₄₁ClN₆O₄Si

There total 10 articles about C₃₂H₄₁ClN₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1364717-24-7
C₂₂H₂₈ClIN₄O₂Si

: 1364718-66-0
C₁₀H₁₄N₂O₂

: 1364718-73-9
C₃₂H₄₁ClN₆O₄Si

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

Reference yield:

: 1364717-17-8
C₂₂H₂₉ClN₄O₂Si

: 1364718-73-9
C₃₂H₄₁ClN₆O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere

1.2: 0.5 h / 60 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

With N,N,N,N,-tetramethylethylenediamine; caesium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1364718-12-6
C₉H₉BrNO₂^(1-)*Na⁽¹⁺⁾

: 1364718-73-9
C₃₂H₄₁ClN₆O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / water / 0.17 h / 20 °C / Cooling with ice

2.1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 1.83 h / 20 - 70 °C

2.2: 10 h / 110 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.2: 1 h / 0 °C

4.1: 1,10-Phenanthroline; copper(l) iodide; caesium carbonate / toluene / 5.5 h / 130 °C / Microwave irradiation

5.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

6.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

With hydrogenchloride; copper(l) iodide; 1,10-Phenanthroline; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;