1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

Base Information

Chemical Name:1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid
CAS No.:104422-88-0
Molecular Formula:C₆₀H₅₅NO₁₃
Molecular Weight:998.096
Hs Code.:

1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

Synonyms:1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

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Chemical Property of 1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

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Technology Process of 1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

There total 13 articles about 1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104423-00-9
6-methoxy-4,5,8,9-tetrakis(phenylmethoxy)naphtho<2,3-c>furan-1,3-dione

: 104422-96-0
3-(diethoxymethyl)-2,8-dihydro-9-(methoxymethoxy)-1H-cyclopentisoquinolin-1-one

: 104422-88-0
1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1021/ja00282a042

Reference yield:

: 40731-98-4
4-hydroxy-2,3-dihydroindan-1-one

: 104422-88-0
1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

3: n-Bu₄NF

4: 82 percent / o-O₂NC₆H₄SeCN, n-Bu₃P, H₂O₂

5: t-BuLi / tetrahydrofuran / 0.5 h / -78 °C

With ortho-nitrophenyl selenocyanate; tributylphosphine; tetrabutyl ammonium fluoride; dihydrogen peroxide; tert.-butyl lithium; In tetrahydrofuran;
DOI:10.1021/ja00282a042

Reference yield:

: 6136-93-2
2,2-diethoxyacetonitrile

: 104422-88-0
1,4,5,8-Tetrakis-benzyloxy-3-{[7-diethoxymethyl-4-methoxymethoxy-5-oxo-5,6-dihydro-6-aza-cyclopenta[b]naphthalen-(1Z)-ylidene]-hydroxy-methyl}-7-methoxy-naphthalene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

2: t-BuLi / tetrahydrofuran / 0.5 h / -78 °C

With tert.-butyl lithium; In tetrahydrofuran;
DOI:10.1021/ja00282a042