diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

Base Information

Chemical Name:diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate
CAS No.:153690-16-5
Molecular Formula:C₂₄H₂₅NO₇
Molecular Weight:439.465
Hs Code.:

Synonyms:diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

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Technology Process of diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

There total 1 articles about diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 153690-15-4
1-(3,4-dimethoxyphenyl)-4-phenyl-3-(trimethylsilyl)azetidin-2-one

: 153690-16-5
diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

Guidance literature:: DOI:10.1002/hlca.19930760820

Reference yield: 76.0%

: 153690-16-5
diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

: diethyl trans-1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylspiro-3',3'-dicarboxylate

Guidance literature:: With potassium hydroxide; dihydrogen peroxide; tetrabutylammomium bromide; In dichloromethane;
DOI:10.1002/hlca.19930760820

Reference yield:

: 1774-47-6
trimethylsulfoxonium iodide

: 153690-16-5
diethyl 2-<1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylazetidin-3-ylidene>propanedioate

: diethyl trans-1-(3,4-dimethoxyphenyl)-2-oxo-4-phenylspiro-2',2'-dicarboxylate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 20 min, r.t., 2.) DMF, THF, r.t.;
DOI:10.1002/hlca.19930760820