(R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate

Base Information

Chemical Name:(R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate
CAS No.:1416352-41-4
Molecular Formula:C₂₅H₃₁NO₄
Molecular Weight:409.525
Hs Code.:

Synonyms:(R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate

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Technology Process of (R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate

There total 1 articles about (R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 62563-07-9
2-(3-bromopropyl)-1,3-dioxolane

: 1416352-41-4
(R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate

Guidance literature:: With cesiumhydroxide monohydrate; (11bR)-(-)-4,4-dibutyl-4,5-dihydro-2,6 bis(3,4,5-trifluorophenyl)-3H-dinaphth[2,1-c:1’,2’-e]azepinium bromide; In toluene; at -40 ℃; for 16h; enantioselective reaction;
DOI:10.1039/c2ob26778k

Reference yield: 75.0%

: 1416352-41-4
(R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate

: 140646-13-5
tert-butyl 2(R)-piperidinecarboxylate

Guidance literature:: (R)-tert-butyl 5-(1,3-dioxolan-2-yl)-2-(diphenylmethyleneamino)pentanoate; With trifluoroacetic acid; In ethanol; water; at 20 ℃; for 1h;

With palladium 10% on activated carbon; hydrogen; In ethanol; water; at 40 ℃; for 24h; stereoselective reaction;
DOI:10.1039/c2ob26778k