4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

Base Information

Chemical Name:4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione
CAS No.:1427000-82-5
Molecular Formula:C₃₃H₃₇NS₂
Molecular Weight:511.795
Hs Code.:

Synonyms:4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

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Chemical Property of 4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

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Technology Process of 4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

There total 3 articles about 4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1427000-64-3
4,5,6,7-tetrahydro-3-(2,6-dibromophenyl)-(3H)-benzothiazole-2-thione

: 560132-24-3
3-tert-butylphenylboronic acid

: 1427000-82-5
4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

Guidance literature:: With palladium diacetate; cesium fluoride; johnphos; In tetrahydrofuran; at 50 ℃; for 8h; Inert atmosphere;

Reference yield:

: 608-30-0
2,6-dibromoaniline

: 1427000-82-5
4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; dimethyl sulfoxide / 0.17 h / 5 °C / Inert atmosphere

1.2: 1 h / 5 - 20 °C / Inert atmosphere

2.1: johnphos; cesium fluoride; palladium diacetate / tetrahydrofuran / 8 h / 50 °C / Inert atmosphere

With palladium diacetate; cesium fluoride; sodium hydroxide; johnphos; In tetrahydrofuran; water; dimethyl sulfoxide;

Reference yield:

: 822-87-7
2-Chlorocyclohexanone

: 1427000-82-5
4,5,6,7-tetrahydro-3-[2,6-bis(3-tert-butylphenyl)phenyl]-2(3H)-benzothiazole-thione

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; dimethyl sulfoxide / 0.17 h / 5 °C / Inert atmosphere

1.2: 1 h / 5 - 20 °C / Inert atmosphere

2.1: johnphos; cesium fluoride; palladium diacetate / tetrahydrofuran / 8 h / 50 °C / Inert atmosphere

With palladium diacetate; cesium fluoride; sodium hydroxide; johnphos; In tetrahydrofuran; water; dimethyl sulfoxide;