Technology Process of C36H26O6
There total 5 articles about C36H26O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen bromide; acetic acid;
at 160 ℃;
for 16h;
DOI:10.1021/ma201599p
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(l) chloride / 1-methyl-pyrrolidin-2-one / 22 h / 165 °C / Inert atmosphere
2.1: hydrogen bromide; acetic acid / 16 h / 160 °C / Air atmosphere
3.1: 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / Inert atmosphere
3.2: 22 h / 170 °C / Inert atmosphere
4.1: hydrogen bromide; acetic acid / 16 h / 160 °C
With
2,2,6,6-tetramethylheptane-3,5-dione; hydrogen bromide; caesium carbonate; acetic acid; copper(l) chloride;
In
1-methyl-pyrrolidin-2-one;
1.1: Ullmann condensation / 3.2: Ullmann condensation;
DOI:10.1021/ma201599p
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen bromide; acetic acid / 16 h / 160 °C / Air atmosphere
2.1: 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / Inert atmosphere
2.2: 22 h / 170 °C / Inert atmosphere
3.1: hydrogen bromide; acetic acid / 16 h / 160 °C
With
2,2,6,6-tetramethylheptane-3,5-dione; hydrogen bromide; caesium carbonate; acetic acid;
In
1-methyl-pyrrolidin-2-one;
2.2: Ullmann condensation;
DOI:10.1021/ma201599p
